Microstructural stability of 316 L produced by additive manufacturing for nuclear applications

Additive manufacturing (AM) represents a quite interesting technology for manufacturing components of nuclear reactors. This work investigated the microstructural stability of 316 L steel fabricated via Laser Powder Bed Fusion (L-PBF) from room temperature to 650 degrees C. Despite the reduced susceptibility of the material to sensitization owing to its low carbon content, temperature variations may induce deleterious effects in nuclear safety-critical components. In as-printed condition, the microstructure is not stable and undergoes significant changes induced by thermal cycling up to 650 degrees C in Mechanical Spectroscopy (MS) tests: the typical melt-pool pattern disappears, a population of equiaxed grains substitutes the original ones elongated in the build direction, the average size of the cells forming a finer sub-structure inside the grains increases, texture changes, and the excess of vacancies induced by the rapid cooling is recovered. Although the current literature reports that the microstructure is stable up to 500 degrees C, MS results indicate that the aforesaid irreversible phenomena start at a lower temperature (similar to 230 degrees C). The present results suggest that the microstructure of the printed material must be stabilized through suitable heat treatments before its application in structural components for nuclear reactors.