Solid-state nuclear magnetic resonance (NMR) spectroscopic analysis were carried out on recent and archaeological wood. Cross-polarization-magic-angle spinning C-13 NMR spectra obtained from samples of poplar (Popolus sp.), oak (Quercus sp.), and silver fir (Abies alba) were examined in this study. The most relevant peaks were assigned according to the extensive literature in the area, and the differences observed discussed in terms of lignin and cellulose composition: by fixing a lignin reference signal intensity, the cellulose and hemicellulose moieties showed a strong depletion compared to the lignin signals in archaeological wood.
Alesiani, M., Proietti, F., Capuani, S., Paci, M., Fioravanti, M., Maraviglia, B. (2005). 13C CPMAS NMR spectroscopic analysis applied to wood characterization. APPLIED MAGNETIC RESONANCE, 29(2), 177-184.
13C CPMAS NMR spectroscopic analysis applied to wood characterization
PACI, MAURIZIO;
2005
Abstract
Solid-state nuclear magnetic resonance (NMR) spectroscopic analysis were carried out on recent and archaeological wood. Cross-polarization-magic-angle spinning C-13 NMR spectra obtained from samples of poplar (Popolus sp.), oak (Quercus sp.), and silver fir (Abies alba) were examined in this study. The most relevant peaks were assigned according to the extensive literature in the area, and the differences observed discussed in terms of lignin and cellulose composition: by fixing a lignin reference signal intensity, the cellulose and hemicellulose moieties showed a strong depletion compared to the lignin signals in archaeological wood.I documenti in IRIS sono protetti da copyright e tutti i diritti sono riservati, salvo diversa indicazione.
